Metrika

  • citati u SCIndeksu: 0
  • citati u CrossRef-u:0
  • citati u Google Scholaru:[]
  • posete u poslednjih 30 dana:18
  • preuzimanja u poslednjih 30 dana:5

Sadržaj

članak: 1 od 1  
2020, vol. 47, br. 1, str. 43-53
Brza spektrofotometrijska metoda za određivanje reaktivnih supstanci tiobarbiturne kiseline (TBARS) u hrani za kalifornijske pastrmke
aInstitut za prehrambene tehnologije, Novi Sad
bUniverzitet u Ljubljani, Biotehnički fakultet, Domžale, Slovenija

e-adresasladjana.rakita@fins.uns.ac.rs
Projekat:
Istraživanje savremenih biotehnoloških postupaka u proizvodnji hrane za životinje u cilju povećanja konkurentnosti, kvaliteta i bezbednosti hrane (MPNTR - 46012)

Ključne reči: hrana za ribe; reaktivne supstance tiobarbiturne kiseline; lipidna peroksidacija; validacija metode
Sažetak
Oksidativne promene u hrani za ribe nastale tokom skladištenja predstavljaju veliki problem u ishrani riba. Ovo istraživanje ima za cilj da predstavi brzu i jednostavnu metodu za određivanje reaktivnih supstanci tiobarbiturnekiseline (TBARS) bez hidrolize u komercijalnoj hrani za kalifornijeske pastrmke, kao metodu za određivanje lipidne peroksidacije. Metoda je validovana i ispitane su sledeće karakteristike: linearnost (opseg), granica detekcije, granica kvantifikacije, preciznost (ponovljivost i unutar laboratorijska reproduktivnost), tačnost i stabilnost metode (Xi Rkontrolne karte). Prikazani rezultati ukazuju da je TBARS metoda linearna u opsegu 1.11-13.33 nmol/mL i precizna u uslovima ponovljivosti i unutar laboratorijske reproduktivnosti. S obzirom na malu koncentraciju analita u uzorku metoda je pokazala zadovoljavajuću tačnost. Takođe, metoda je stabilna u pogledu promenljivosti srednjih vrednosti merenja i razlika između merenja. Rezultati dobijeni ovim istraživanjem su ukazali da se ova metoda može uspešno primeniti za određivanje TBARS-a u hrani za kalifornijske pastrmke tokom rutinske kontrole kvaliteta u akvakulturi kada je potrebno analizirati veliki broj uzoraka za kratko vreme.
Reference
AOAC International (2000) Method Validation Programs (OMA/PVM Department), including Appendix D: Guidelines for collaborative study procedures to validate characteristics of a method of analysis. http://www.aoac.org/aoac_prod_imis/AOAC_Do cs/StandardsDevelopment/Collaborative_Study Validation_Guidelines.pdf
Ayala, A., Muñoz, M.F., Argüelles, S. (2014) Lipid Peroxidation: Production, Metabolism, and Signaling Mechanisms of Malondialdehyde and 4-Hydroxy-2-Nonenal. Oxidative Medicine and Cellular Longevity, 2014: 1-31
Bahrevar, R., Faghani-Langroudi, H. (2015) Effect of fish meal replacement by blood meal in fingerling rainbow trout (Oncorhynchus mykiss) on growth and body/fillet quality traits. Aquaculture, Aquarium, Conservation & Legislation: International Journal of the Bioflux Society, 8(1): 34-39
Barriuso, B., Astiasarán, I., Ansorena, D. (2013) A review of analytical methods measuring lipid oxidation status in foods: A challenging task. European Food Research and Technology, 236(1): 1-15
Beljkaš, B., Matić, J., Milovanović, I., Jovanov, P., Mišan, A., Šarić, L. (2010) Rapid method for determination of protein content in cereals and oilseeds: Validation, measurement uncertainty and comparison with the Kjeldahl method. Accreditation and Quality Assurance, 15(10): 555-561
Botsoglou, N.A., Fletouris, D.J., Papageorgiou, G.E., Vassilopoulos, V.N., Mantis, A.J., Trakatellis, A.G. (1994) Rapid, Sensitive, and Specific Thiobarbituric Acid Method for Measuring Lipid Peroxidation in Animal Tissue, Food, and Feedstuff Samples. Journal of Agricultural and Food Chemistry, 42(9): 1931-1937
Esterbauer, H., Cheeseman, K.H. (1990) Determination of aldehydic lipid peroxidation products: Malonaldehyde and 4-hydroxynonenal. Methods in Enzymology, 186, 407-421
EURACHEM (2014) The fitness for purpose of analytical methods: A laboratory guide to method validation and related topics. Teddington, Middlesex, UK: LGC
European Commission (2002) Commission decision 2002/657/EC of 12 August 2002 implementing Council Directive 96/23/EC concerning the performance of analytical methods and the interpretation of results. Official Journal of the European Union, L221, 8-36
Gustavo, G.A., Ángeles, H.M., Asuero, A.G. (2010) Intra-laboratory assessment of method accuracy (trueness and precision) by using validation standards. Talanta, 82(5): 1995-1998
Hamre, K., Kolås, K., Sandnes, K., Julshamn, K., Kiessling, A. (2001) Feed intake and absorption of lipid oxidation products in Atlantic salmon (Salmo salar) fed diets coated with oxidised fish oil. Fish Physiology and Biochemistry, 25: 209-219
Hamre, K., Kolås, K., Sandnes, K. (2010) Protection of fish feed, made directly from marine raw materials, with natural antioxidants. Food Chemistry, 119(1): 270-278
Hessel, V., Hardt, S., Löwe, H. (2006) Chemical micro process engineering: Fundamentals, modelling and reactions. New Jersey, US: John Wiley & Sons
Hevrøy, E.M., Sandnes, K., Hemre, G.I. (2004) Growth, feed utilisation, appetite and health in Atlantic salmon (Salmo salar L.) fed a new type of high lipid fish meal, Sea Grain®, processed from various pelagic marine fish species. Aquaculture, 235(1-4): 371-392
Horwitz, W. (2003) Validation: An invisible component of measurement. Gaithersburg, MD: AOAC International
Ionescu, J.G., Poljsak, B. (2010) Metal ions mediated pro-oxidative reactions with vitamin C: Possible implications for treatment of differrent malignancies. International Journal of Cancer Prevention, 3(3): 149-174
Laohabanjong, R., Tantikitti, C., Benjakul, S., Supamattaya, K., Boonyaratpalin, M. (2009) Lipid oxidation in fish meal stored under different conditions on growth, feed efficiency and hepatopancreatic cells of black tiger shrimp (Penaeus monodon). Aquaculture, 286(3-4): 283-289
Mendes, R., Cardoso, C., Pestana, C. (2009) Measurement of malondialdehyde in fish: A comparison study between HPLC methods and the traditional spectrophotometric test. Food Chemistry, 112(4): 1038-1045
Papastergiadis, A., Mubiru, E., van Langenhove, H., de Meulenaer, B. (2012) Malondialdehyde Measurement in Oxidized Foods: Evaluation of the Spectrophotometric Thiobarbituric Acid Reactive Substances (TBARS) Test in Various Foods. Journal of Agricultural and Food Chemistry, 60(38): 9589-9594
Rakita, S., Pojić, M., Tomić, J., Torbica, A. (2014) Determination of free sulphydryl groups in wheat gluten under the influence of different time and temperature of incubation: Method validation. Food Chemistry, 150(1): 166-173
Seljeskog, E., Hervig, T., Mansoor, M.A. (2006) A novel HPLC method for the measurement of thiobarbituric acid reactive substances (TBARS): A comparison with a commercially available kit. Clinical Biochemistry, 39(9): 947-954
Taverniers, I., de Loose, M., van Bockstaele, E. (2004) Trends in quality in the analytical laboratory: Analytical method validation and quality assurance. TrAC Trends in Analytical Chemistry, II, 23(8): 535-552
Tomažin, U., Frankič, T., Voljč, M., Rezar, V., Levart, A., Salobir, J. (2013) The potency of a-and g-tocopherol, and their combination, in reducing dietary induced oxidative stress in vivo and improving meat lipid stability in broilers. European Poultry Science, 77(4): 266-274
Ullah, A.A.K.M., Maksud, M.A., Khan, S.R., Lutfa, L.N., Quraishi, S.B. (2017) Development and validation of a GF-AAS method and its application for the trace level determination of Pb, Cd, and Cr in fish feed samples commonly used in the hatcheries of Bangladesh. Journal of Analytical Science and Technology, 8(1): 1-7
Voljč, M., Frankič, T., Levart, A., Nemec, M., Salobir, J. (2011) Evaluation of different vitamin E recommendations and bioactivity of a-tocopherol isomers in broiler nutrition by measuring oxidative stress in vivo and the oxidative stability of meat. Poultry Science, 90(7): 1478-1488
Watanabe, J., Oki, T., Takebayashi, J., Yamasaki, K., Takano-Ishikawa, Y., Hino, A., Yasui, A. (2012) Method Validation by Interlaboratory Studies of Improved Hydrophilic Oxygen Radical Absorbance Capacity Methods for the Determination of Antioxidant Capacities of Antioxidant Solutions and Food Extracts. Analytical Sciences, 28(2): 159-165
Watanabe, J., Takebayashi, J., Takano-Ishikawa, Y., Yasui, A. (2012) Evaluation of a Method to Quantify Quercetin Aglycone in Onion (Allium cepa) by Singleand Multi-laboratory Validation Studies. Analytical Sciences, 28(12): 1179-1182
Wild, C.J., Seber, G.A.F. (2000) Change encounters: A first course in data analysis and inference. New York: John Wiley & Sons
Wold, J.P., Kvaal, K. (2000) Mapping Lipid Oxidation in Chicken Meat by Multispectral Imaging of Autofluorescence. Applied Spectroscopy, 54(6): 900-909
Yildiz, M., Köse, İ., Issa, G., Kahraman, T. (2015) Effect of different plant oils on growth performance, fatty acid composition and flesh quality of rainbow trout (Oncorhynchus mykiss). Aquaculture Research, 46(12): 2885-2896
Zeb, A., Ullah, F. (2016) A Simple Spectrophotometric Method for the Determination of Thiobarbituric Acid Reactive Substances in Fried Fast Foods. Journal of Analytical Methods in Chemistry, 2016(5): 1-5
 

O članku

jezik rada: engleski
vrsta rada: originalan članak
DOI: 10.5937/FFR2001043R
objavljen u SCIndeksu: 04.07.2020.
metod recenzije: jednostruko anoniman
Creative Commons License 4.0